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RECOVERY OFBUTANOL FROM A MIXTURE OF BUTANOL 2011

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RECOVERY OFBUTANOL FROM A MIXTURE OF BUTANOL 2011 ( recovery-ofbutanol-from-mixture-butanol-2011 )

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US 2011/0162954A1 Jul.7,2011 TABLE 8 Simulated Solvent Column Tral?c and Liquid Mass Composition Pro?le Outputs for Example 2. Heat Liquid Vapor Liquid Vapor Temperature Pressure duty ?oW ?oW feed feed Stage C. atm MJ/hr kghr kg/hr kghr kghr 26040.818 41144.65 22607.57 1.0376553 21430.278 44576.86 0 736.68398 1 88.9422712 2 89.1928695 3 92.0459809 4 92.3323703 5 92.517813 1.015121 0 6 92.7125512 7 92.9575427 8 93.4298808 9 94.72859 1.043319 0 10 97.4651369 11 100.068667 12 101.327321 13 101.844136 14 102.120204 15 102.329061 1.050368 0 1.057418 0 1.064467 0 1.071517 0 1.078566 0 1.0856165155.09 Stage 4754.139 OLEYLOH 5.14E-07 0.000277 0.494574 0.494288 0.494232 0.494724 0.497686 0.510144 0.542861 0.580035 0.598525 0.604357 0.605871 0.60618 0.889041 rectifying section at an introduction point above the strippingsection,the?rstdistillationcolumnhavingan operating temperature, T1 and an operating pressure P l at a predetermined point in the stripping section, Wherein T 1and P 1are selected to produce a ?rst bottoms stream and a ?rst vaporous overhead stream, the ?rst bottoms stream comprising the Water-immiscible OrganicextractantandWaterandbeingsubstantiallyfree ofbutanol, and the ?rstvaporous overhead stream com 1 0.441665 2 0.2485 3 0.261893 4 0.262119 5 0.262003 6 0.26068 7 0.253908 8 0.226084 9 0.152452 10 0.066076 11 0.020756 12 0.005693 13 0.001485 14 0.00037 15 0.0001 0.986923 0 0.993973 0 1.001022 0 1.008072 0 94496.221 39229.63 70360.43 0 0 0 0 0 0 0 0 0 0 0 0 0 1.022171 0 1.02922 0 1.036269 0 94550.968 41935.15 94561.975 41989.89 94468.264 42000.9 93907.442 41907.19 91619.38 41346.37 86109.931 39058.3 80604.9 33548.86 78122.027 28043.82 77370.843 25560.95 77178.529 24809.77 77139.76 24617.45 52561.076 24578.68 0 0 0 0 0 0 0 0 0 0 0 0 1st Mixed Liquid Vapor liquid liquid f6?® proc@ prc® f® ?oW Stage kg/hr kg/hr kg/hr kg/hr kg/hr 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 IiBUOH 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 52561.076 WATER 0.558303 0.751206 0.243518 0.243593 0.243765 0.244596 0.248406 0.263772 0.304687 0.35389 0.380719 0.38995 0.392644 0.39345 0.110859 41144.65 12648.19 13392.63 @ indicatestextmissingorillegibleWhen?led What isclaimedis: 1.A processcomprisingthesteps: a) introducing a feed comprising: (i)aWater-immiscibleorganicextractant, (ii) Water, (i)atleastone isomer ofbutanol, and (iv)optionallyanon-condensablegas intoa?rstdistillationcolumn,Whereinthe?rstdistillation column comprises a stripping section and optionally a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 CO2 3.21E-05 1.72E-05 1.50E-05 9.58E-08 6.16E-l0 3.97E-12 2.55E-14 0 0 0 0 0 0 0 0 4325.494 17104.78 75947.21 75986.38 75975.56 75792.34 74839.89 71058.04 62124.16 53428.86 49511.75 48282.81 47946.52 47859.93 47806.94 18549.01 18564.59 18586.42 18675.92 19067.55 20561.34 23985.77 27176.04 28610.28 29088.03 29232.01 29279.83 2nd

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