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Formation and detection of (DHA)2 HPLC-MS of a cycled DHAQ electrolyte after a strongly oxidative discharge (+350 mV) was applied, showing disappearance of DHA and the appearance of new compounds with [M-H]- = 449.1028 and [M-H]- = 223.0404. a Figure S7. (a) LC-MS trace of DHAQ after prolonged cycling shows disappearance of the DHA peak and appearance of an additional peak at 10.2 min with [M-H]- of 449.1028. (b) Mass spectrum of the material eluted at 10.2 min in the LC trace. A [M-H]- of 449.1028 corresponds to a neutral molecular formula C28H18O6. The majority of the ions existed in a fragment with [M-H]- of 223.04104. (c) The material with [M-H]-of 449.1028 was isolated and fragmented by MS/MS, indicating that the signal with [M-H]- of 223.04104 observed by LC-MS corresponds to fragments of the material with [M-H]-of 449.1028. b c MS/MS of m/z = 449 9PDF Image | Extending organic flow batteries via redox state management
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