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Identification of (DHA)2 A sample with [M-H]- of 449.1028 was isolated from the DHAQ electrolyte by pHPLC (preparative HPLC), and its mass and retention time were confirmed by LC-MS. The structures were subsequently assigned as (DHA)2 stereoisomers by NMR. a b Figure S8. LC-MS traces of (a) DHAQ after pHPLC separation of cycled DHAQ electrolyte and (b) DHA dimers (DHA)2 after pHPLC separation. (DHA)2 is pure by LC trace: The peaks at 7.38 min and 10.83 min are due to impurities from solvents and were also present in blank samples. 10PDF Image | Extending organic flow batteries via redox state management
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