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Chapter 6. Electrochemical Impedance of Single Flow Cells Figure 6.12: (a) Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1 M K4[Fe(CN)6] dissolved in 1 M KCl adjusted to pH 12 with KOH. The impedance was recorded from 100 kHz to 100 mHz at a flow rate of 50 mL min−1 and controlled temperatures ranging from 31◦C to 35◦C. (b) Same as in (a) but shifted by 0 Ω cm2, 0.023 Ω cm2, 0.039 Ω cm2, 0.056 Ω cm2, and 0.072 Ω cm2 along the real axis (in the order 31 ◦C to 35 ◦C). Figure 6.13: Results from the CNLS fit of the 0.1 M/0.1 M ferri-/ferrocyanide impedance recorded at 31 ◦C presented in Figure 6.12. (a) Experimental and modelled Nyquist plots. (b) Experimental and modelled semi-logarithmic Bode plots of the imaginary impedance. (c) Kramers-Kronig test residuals. (d) Relative fit residuals. 100PDF Image | Organic Redox Flow Batteries 2023
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