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a) b) c) d) e) 100 95 90 85 80 300 400 500 600 700 800 CF@TiO2 CF@TiO2 N500 CF@TiO2 N700 CF@TiO2 N900 Wavelength / nm Figure 6.28 - Images, taken from Carl-Zeiss optical lens, of the electrodes after their respectively treatment: a) CF@TiO2; b) CF@TiO2 N500; c) CF@TiO2 N700 d) CF@TiO2 N900 e) UV-vis Absorption spectra for CF@TiO2, CF@TiO2 N500, CF@TiO2 N700 and CF@TiO2 N900. 6.1.3.1.3 Electrochemical characterization After study the chemical modification of the different electrodes, cyclic voltammetry (CV) was done as electrochemical analysis towards V2+/V3+ redox reaction (Table 6.4). Several electrochemical observations can be made from the CV (Figure 6.29a). It is clearly evidenced the poor electrocatalytic activity of the CF towards 116 Absorbance / %PDF Image | Redox Flow Batteries Vanadium to Earth Quinones
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