THERMAL ENERGY STORAGE USING PARAFFIN WAX

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THERMAL ENERGY STORAGE USING PARAFFIN WAX ( thermal-energy-storage-using-paraffin-wax )

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Figure 3.12: Temperature profile of the center bottom thermocouple at different flow directions with 4 LPM during charging at 75°C................................................................47 Figure 3.13: Temperature profile of the center bottom thermocouple at different inlet positions with 1 LPM during discharging at 20°C.............................................................48 Figure 4.1: A: Paraffin wax, B: MWCNTs, C: Al2O3, D: GNPs. E: Sodium oleate, F: Octadecylamine..................................................................................................................52 Figure 4.2: Sample preparation using the mechanical dispersion method.........................52 Figure 4.3: KD2 Pro Thermal Conductivity Analyzer and its sensors: TR-1, KS-1, SH-1 (from left to right). .............................................................................................................55 Figure 4.4: Thermal conductivity change in liquid phase (60°C) over time after sample preparation. ........................................................................................................................56 Figure 4.5: 3-D printed mold for thermal conductivity measurements in solid phase.......57 Figure 4.6: Picture of each sample after being removed from the mold............................57 Figure 4.7: Thermal conductivity change of MWCNT-wax samples with temperature. ..59 Figure 4.8: Thermal conductivity change of GNP-wax samples with temperature...........59 Figure 4.9: Thermal conductivity change of Al2O3-wax samples with temperature........60 Figure 4.10: Mettler-Toledo DSC1, Differential Scanning Calorimeter. ..........................63 Figure 4.11: DSC heating and cooling curves of paraffin wax with MWCNT, GNP and Al2O3 nanoparticles at different concentrations.................................................................63 Figure 4.12: Stability observation of MWCNT-wax samples in liquid phase over first (1), second (2) and, third (3) melting/solidification cycles (Sample A: 0.1 wt.%, 100 min sonication; B: 0.1 wt.%, 40 min sonication; C: 0.075 wt.%, 70 min sonication, D: 0.05 wt.%, 100 min sonication, E: 0.05 wt.%, 40 min sonication)............................................66 viii

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