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(a) Nanotube networks (b) Carbon-derived carbons (c) Carbon-derived carbons produced at 600°C produced at 1200°C Figure 16. Atomic simulation of 3D ordered architectures (a) and disordered architectures (b) and (c). Source: Refs. 4 and 7. Additional sorption specificity may be achieved by modifying the surface of a sorbent— either on a particle or in a pore. If specific functional groups are added to a structure, enhanced sorption and release mechanisms can be employed, including those that use external release triggers, such as applied fields. Beyond simple porous materials, many types of “designer structures” could be imagined to enhance sorption/release processes. For example, it has been demonstrated recently that combining the inherent rigidity of MOFs and the functional flexibility of polymers can create a large number of single-phase materials, each of which has multivariate functionalities (Figure 17). The properties of multivariate MOFs are not simple linear combinations of their constituents; this supports the notion that the sequence of functionalities within a porous network may well be useful as code for enhancing a specific property or achieving a new property.8 Another approach to increasing the selectivity of solid sorption separation is to introduce coatings to sorbent materials by depositing a continuous, thin, conformal coating onto high- specific-surface-area substrates. For example, introducing metal or oxide nanoparticles and clusters with terminal functionality to a sorbent in a controlled manner has the potential to control CO2 sorption. Again, the goal is to enhance the uptake and control the release of a targeted gas, taking advantage of various processes such as using external stimuli to affect release, decreasing the activation energy, Figure 17. Multivariate MOF-5 structure with eight different functionalities. Source: Ref. 8. 60PDF Image | 2020 Carbon Capture
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