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Additional (unpublished) graphs, data, materials and photos of Performance Data (delineating Sect. 4 of the submitted 25 page C2CNT written Submission) Initial demonstrations of operation included in this description are the of carbon dioxide’s extraordinarily rapid rate of carbon dioxide absorption from the gas phase into molten lithium carbonate and molten lithium carbonate mixtures was experimentally determined and documented. Even the lowest carbon dioxide concentrations studied (0.04% CO2 using conventional air) is sufficient to maintain and renew all molten lithium carbonate in an open air system during electrolyses conducted at constant current density of 0.1 A/cm2. During the electrolysis, lithium oxide is co-generated at the cathode, which reacts with carbon dioxide continuously renewing the electrolyte. As demonstrated in the figure below, the rate of carbon dioxide absorption bubbled into even a small amount (50 g) of molten lithium carbon dioxide gas is not limited until the flow rates is well over 0.3 liters CO2 per minute, and as expected (not shown) further increases with added lithium oxide concentration. The CO2 cumulative absorbed on the vertical axis is limited to just below 100% due to the natural lithium oxide concentration which occurs on equilibrium with the lithium carbonate electrolyte (as we have measured in reference 11 on page 3 in the above section). After the measurements shown, it was noted that the calibration of the Omega CO2 controller calibration to measure and control CO2 flow rate had slipped downward, and the limiting Cumulative CO2 absorbed is higher than the indicated 92%. During the most rapid rate of C2CNT production tested of 1amp/cm2, gas containing CO2 must be bubbled into the electrolyte, otherwise electrolyte would be consumed and the level of electrolyte visibly falls under those circumstances with bubbling a constant mass of electrolyte is maintained during the electrolysis. Experimental data Electrolyte Crucible Temp, C CO2 flow rate, mL/min CO2 inlet temperature CO2 inlet flow measurements Results 50 g Li2CO3 + 1 m Li2O Alumina, 100 mL 770 60-600 mL/min Room temperature (no pre-heating) Alumina tube: 1-bore (ID=3mm), sparger Weight of crucible measured every 5 (or10 min), no electrolysis A large series of experiments conducted by C2CNT demonstrated that a wide range of interesting and useful carbon nanotubes can be uniformly formed by varying the molten carbonate composition, and the inexpensive metals used for the carbon nanotube generating cathode and the oxygen generating anode. This is extensively, scientifically, photo documented in the references 1 through 11 on pages 2 and 3, and in the C2CNT scientific articles attached with the submission. 4PDF Image | Xprize
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