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Nanomaterials 2020, 10, 555 7 of 12 nm are formed. For large silver nanoparticles, an extinction wavelength around 600 nm [45] results, which explains the redshift of the spectrum. For the two longer treated stock solutions, the UV/VIS absorption spectra clearly show the diversity of the resulting particles in shape and size. Nanomaterials 2020, 10, 555 8 of 13 100 nm 100 nm 100 nm 10 nm 10 nm 10 nm (c) Figure 5. Particle size distribution fitted by Gaussian functions with mean particle size and standard (a) (b) Figure 5. Particle size distribution fitted by Gaussian functions with mean particle size and standard deviation illustrated at the top. UV/VIS absorption spectra and characteristics of the particles are deviation illustrated at the top. UV/VIS absorption spectra and characteristics of the particles are shown shown at the bottom with TEM-images in between. On the left-hand side: (a) S2 after plasma at the bottom with TEM-images in between. On the left-hand side: (a) S2 after plasma treatment time treatment time of t = 10 s, in the middle: (b) S2 after t = 30 s, and on the right-hand side: (c) S4 after t = oft=10s,inthemiddle: (b)S2aftert=30s,andontheright-handside: (c)S4aftert=60sareshown. 60 s are shown. By fitting the histogram data with two Gauss functions, conclusions are drawn about the synthesis steps nucleation and particle growth. The two Gauss functions symbolize different size regimes. The first Gauss function describes very small nanoparticles or nuclei with a particle diameter dparticle in the range around 2 nm. The position and width of the first Gauss function arePDF Image | Formation Kinematics of Plasma-Generated Silver Nanoparticles
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