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Process Intensification for the Synthesis of Metal Nanoparticles

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Process Intensification for the Synthesis of Metal Nanoparticles ( process-intensification-synthesis-metal-nanoparticles )

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KHODASHENAS et al., Orient. J. Chem., Vol. 31(Spl Edn.), 249-257 (2015) 255 achieve uniform mixing of the two streams on the rotating disc constituted a considerable processing advantage in producing highly stable particles of about 10 nm and of very narrow distributions 44. Mohammadi et al., (2014) produced titanium dioxide less byproduct formation, (2) chemicals that are dangerous to handle and stored in large quantities, can be produced safely using a microreactor as much as needed, (3) fast reactions which could accelerate uncontrollably in conventional reactors leading to possible explosions, can be run safely Fig. 6: A schematic view of a spinning disk reactor 49 nanoparticles via a sol–gel route on a spinning disc reactor (SDR). They also studied the physical parameters such as rotational speed, disc surface texture, and operating parameters such as flowrate, ratio of water to precursor and location of feed introduction points in terms of their effects on TiO2 particle size, particle size distribution (PSD) and particle yield 48. CONCLUSION Since the wide range of Nano Particles applications in various fields and the need of using the intensification technology in order to minimize plant or equipment size in the synthesis process, reviewing some intensification techniques e.g., Segmented Flow Tubular Reactor, microreactors and spin disc reactor for synthesis process is the main aim of the present paper. Process intensification refers to the intensification of production by increasing the rates of heat and mass transfer by orders of magnitude over conventional stirred batch reactors. Any chemical engineering development that leads to a substantially smaller, cleaner, safer and more energy efficient technology is process intensification 9. The implementation of process intensification techniques resulted in the improvement in green synthesis processes without damaging the environment and requiring less capital cost 7. It was proved that the SFTR is a powerful tool for the production of powders and nanocrystals with advanced. In the past several years microreactors and microprocess engineering have been the subject of worldwide academic research. Microreactor technology has the ability to control the reactions at the micrometer scale. Synthesis in microreactors has several important advantages over conventional batch process synthesis. They include: (1) small volumes and short paths cause more uniform processing conditions and result in

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