Solids handling for intensified process technology

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Solids handling for intensified process technology ( solids-handling-intensified-process-technology )

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IbD PU Deliverable 3.1 6 7 5.3 Impinging stream (IS) reactors................................................................................................................................ 42 5.3.1 Grinding in IS reactors............................................................................................................................................................ 43 5.3.2 Drying and milling in IS reactors....................................................................................................................................... 43 5.3.3 Nanoparticle synthesis in IS reactor/RPB hybrid ..................................................................................................... 45 5.3.4 Crystallization in dual impinging jet mixers................................................................................................................ 46 5.4 Mixer-settlers................................................................................................................................................................... 47 MINIATURIZED REACTOR TECHNOLOGIES (MRT) ............................................................................................................. 49 6.1 Continuous flow microreactor.................................................................................................................................. 49 6.2 Catalytic plate reactor................................................................................................................................................. 50 6.3 Compact heat exchanger reactors (HEX reactors)........................................................................................... 52 6.3.1 Plate HEX reactor ...................................................................................................................................................................... 52 6.3.2 Continuous Helix mini reactor ........................................................................................................................................... 53 ELECTROMAGNETIC FIELDS .................................................................................................................................................... 54 7.1 Microwaves ...................................................................................................................................................................... 54 7.1.1 Synthesis of nanoparticles.................................................................................................................................................... 55 7.1.2 Crystallization............................................................................................................................................................................. 55 7.1.3 Drying ............................................................................................................................................................................................. 55 7.1.4 Heterogeneous catalytic reactions ................................................................................................................................... 56 7.2 Ultrasound........................................................................................................................................................................ 56 7.2.1 Nanoparticle preparation ..................................................................................................................................................... 57 7.2.2 Drying ............................................................................................................................................................................................. 57 7.2.3 Anti-fouling .................................................................................................................................................................................. 58 7.3 Radio frequency (R.F.) heating................................................................................................................................. 59 7.4 Electrohydrodynamics and electrostatic spraying........................................................................................... 60 7.5 Electrochemical and photochemical processes ................................................................................................. 61 7.6 Magnetic field.................................................................................................................................................................. 62 7.6.1 Solids-solids separation......................................................................................................................................................... 62 7.6.2 Industrial application of MSB ............................................................................................................................................. 62 7.7 Plasma................................................................................................................................................................................ 63 MULTIFUNCTIONAL REACTORS & HYBRID PI TECHNOLOGIES ......................................................................................... 64 8.1 Reactive distillation ...................................................................................................................................................... 65 8.2 Reactive extraction ....................................................................................................................................................... 66 8.3 Reactive crystallization ............................................................................................................................................... 66 TECHNOLOGIES RELEVANT TO THE IBD® CASE STUDIES ................................................................................................. 67 9.1 Separation ........................................................................................................................................................................ 67 9.1.1 Froth floatation .......................................................................................................................................................................... 67 9.1.2 Particle classification .............................................................................................................................................................. 70 9.2 Grinding............................................................................................................................................................................. 73 9.2.1 Stirred-ball mill.......................................................................................................................................................................... 73 9.3 Milling ................................................................................................................................................................................ 74 9.3.1 Wet-stirred media milling .................................................................................................................................................... 74 8 9 v

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