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Solids handling for intensified process technology

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Solids handling for intensified process technology ( solids-handling-intensified-process-technology )

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IbD PU Deliverable 3.1 liquid feeding, the SDR also has an optional inlet/outlet for a reactive/inert gas stream. The main operational parameters of a SDR of a given disk size are disk rotating speed, feed flow rate, disk temperature, and reactor pressure. Stainless steel and brass are the commonly used materials for the disk because of their higher thermal conductivity compared to plastic materials, a key requirement for rapid heat transfer across the disk. Teflon coated discs have also been applied in precipitation applications in order to control fouling of the disc surface (Oxley et al., 2000). In terms of scale-up potential, a 500 mm diameter disc can typically process about 150 kg/hour of material with water-like viscosity, the flowrate being limited by the maximum film thickness recommended to be typically no more than 300 microns (Boodhoo, 2013). For higher throughput, multi-disc designs operating in parallel is a viable option. Figure 5. Schematic of a typical SDR (Ramshaw and Cook, 2005). The SDR is suitable for gas-liquid, liquid-liquid, liquid-solid, and gas-liquid-solid reactions, especially where excellent mixing is a key requirement. Crystallization by cooling or solvent anti-solvent methods (Oxley et al., 2000) and nanoparticle synthesis by reactive precipitation methods (Cafiero et al., 2002; Tai et al., 2007; Dehkordi and Vafaeimanesh, 2009; de Caprariis et al., 2012; Jacobsen and Hinrichsen, 2012; Mohammadi et al., 2014) are the applications of SDR for solids handling. A selection of the previous research into SDR technology involving solids processing is presented in the following sections. 9

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