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IbD PU Deliverable 3.1 mixing when the reactor body is subjected to lateral shaking (Figure 39). This results in intense mixing without the need for rotating shafts, mixing baffles, or mechanical seals. This method also eliminates the problems associated with centrifugal separation whenever two phases are present. Lab scale reactor cells have typical working capacities from 10 to 100 millilitres whereas the industrial scale reactor tubes’ capacities are typically 1 to 10 litres. The use of dynamic mixers allow for the independence of mixing efficiency upon reactor stage size, shape, or fluid velocity. Tests have shown that the reactors delivered excellent mixing performance with homogeneous fluids, immiscible liquids, slurries, and gas/liquid mixtures, with zero back mixing between reaction stages, which is an ideal plug flow condition (AMTechnology, 2015). Figure 39. A laboratory scale Coflore® agitated cell reactor (ACR) with 10 reaction cells within a monolithic block (Gasparini, 2012). The relatively simple geometry and excellent mixing throughout the Coflore reactors enable an effective means of keeping multiphase mixtures suspended and well dispersed in order to maintain an orderly flow through the reactors. Table 1 compares the performance of Coflore against micro and tubular reactors. Performance-wise, Coflore offers a much reduced pressure drop, which contributes to lower pump costs. It also shows that the length of Coflore is typically less than 1% of a tubular reactor. Short and large diameter tubes are preferred as they are easier to clean and have longer service life (AMTechnology, 2015). 40PDF Image | Solids handling for intensified process technology
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