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IbD PU Deliverable 3.1 Table 1. Performance comparison between micro-, tubular-, and Coflore reactors (AMTechnology, 2015). 5.2.1 Processing of slurry in Coflore® ACR Browne et al. (2011) recently demonstrated the efficacy of industrial-scale Coflore ACR tubes in the continuous production of a slurry, N-iodomorpholine. This hydroiodide salt is formed by the reaction morpholine with iodine. The batch mode often results in a 90% yield. The tests in the ACR, which used a 100 mL reactor block revealed that the slurry was produced relatively quickly and the ACR facilitated the continuous processing of a slurry by ensuring a uniformly dispersed suspension at all times. An optimal scheme (Figure 40) processed the slurry for 9h, giving 208g of solid product with a 94% yield, better than the reported batch mode. The process in the ACR involved very little manual handling i.e. restocking of reagent bottles and solvent waste removal. This demonstrated the suitability for medium scale processing as up to 3.88 kg of material could be obtained for a continuous run of one week. Salt forming reactions are a common process for the preparation of many APIs. This demonstration provides an opportunity for ACRs to be promoted in pharmaceuticals. Figure 40. The optimal flow setup for a continuous production of N-iodomorpholine via Coflore ACR with a 94% yield (Browne et al., 2011). 41PDF Image | Solids handling for intensified process technology
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