Solids handling for intensified process technology

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Solids handling for intensified process technology ( solids-handling-intensified-process-technology )

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IbD PU Deliverable 3.1 5.3.3 Nanoparticle synthesis in IS reactor/RPB hybrid Fan et al. (2016) described an attempt to combine the impinging stream with rotating packed bed in the continuous preparation of Fe3O4 nanoparticles in a pilot plant scale (Figure 45). The feedstocks were aqueous solutions of ferric and ferrous chloride and sodium hydroxide. The variables included: high gravity factor, liquid flow rate, and reactant concentration. The stirred tanks A and B were fed into the IS impingement zone in the middle of the RPB, which further intensified the micro-mixing as the reactants flowed radially outwards. The suspension with the nanoparticles was collected after exiting the RPB and nanoparticle separation was carried out by using a magnetic field. The results showed preference towards high gravity levels (RPB speed up to 1250 rpm) in producing small nanoparticle sizes (7.5-11.3 nm). The production rate reached 2.23 kg/h and scale up to industrial scale was believed to be feasible, in part due to the strong micro-mixing characteristics of the device. Figure 45. Fe3O4 production plant (1) stirred tank, (2) stirred tank, (3) valve, (4) rotameter, (5) IS reactor/rotating packed bed, (6) reservoir, (7) nitrogen cylinder, (8) piezometer (Fan et al., 2016). 45

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