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IbD PU Deliverable 3.1 Figure 48. A basic schematic of a mixer-settler (Anon, 2013). Figure 49. Outotec mixer-settler with VSF® technology (Outotec, 2016). Recently, Lade et al. (2015) carried out tests on a pilot scale combined air-lift mixer settler unit (CAL-MSU), transferring tributyl phosphate (TBP) from an aqueous stream into an organic solvent. The intensification of mass transfer processes was made possible by the introduction of inert gas as a mixing agent thereby forming a tri-phase G-L-L system. CALMIX (the device for the gas introduction) is shown in the plan-view of the CAL-MSU unit (Figure 50). This mode of energy introduction increases the turbulence, which enhances dispersion and coalescence of droplets. As gas passes through a liquid-liquid interface with high velocity through a sparger, the dispersions and emulsions arise as a consequence of liquid displacement by bubbles. Detailed mass transfer coefficient and power requirement tests revealed that energy input per unit volume was found to be two times lower for air-sparged CAL-MSU in comparison with a similar configuration pump-mix mixer-settler unit. 48PDF Image | Solids handling for intensified process technology
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