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Nanomaterials 2020, 10, 1321 4 of 15 The productivity P [kg/d] was calculated as the multiplication of the total flowrate (converted in l/d), initial Zn concentration (converted in kg/L), and yield of ZnO. Table 1. Experimental conditions adopted in the 25 runs. ID QZn (L/min) 25 QKOH (L/min) 25 50 100 Zn(II) (M) 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.2 0.1 0.05 0.5 1 0.5 0.75 1 2 KOH (M) 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.8 0.4 0.2 2 4 2 3 4 8 ω (rpm) 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 200 400 800 1200 1400 1400 1400 1400 1400 1400 1400 1400 1400 ri (cm) 1.5 1.5 1.5 2 2 2 2.5 2.5 2.5 3 3 3 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 1 2 3 4 5 6 100 7 25 8 50 9 100 10 25 11 50 12 100 13 50 14 50 15 50 16 50 17 50 18 50 19 50 20 50 21 50 22 500 23 500 24 500 25 500 50 100 25 25 50 50 100 25 50 100 25 50 100 50 50 50 50 50 50 50 50 50 500 500 500 500 3. Results In this section, the experimental results of the 25 runs will be reported. A summary table (Table 1) of the investigated operating conditions is reported. 3.1. Influence of Reagents Flowrate and Reagent Injection Point Position Figure 2 repots the average diameter of nZnO as a function of different QZn (i.e., QKOH) and ri values. Table 2 reports the detail of the results obtained in the first 12 runs. Table 2. Results obtained in the first 12 runs. ID 1 2 3 4 5 6 7 8 9 QZn (L/min) 25 QKOH (L/min) 25 0.02 KOH (M) 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 w (rpm) 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 1400 ri (cm) 1.5 1.5 1.5 2 2 2 2.5 2.5 2.5 3 3 3 d (nm) Yield 84.2 0.961 67.1 0.956 74.3 0.949 81.3 0.980 64.1 0.972 69.5 0.966 69.1 0.982 50.3 0.979 55.7 0.968 76.4 0.961 59.4 0.956 63.7 0.952 P (kg/d) 0.113 0.224 0.445 0.115 0.228 0.453 0.116 0.229 0.454 0.116 0.230 0.456 PSD 1 Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal Unimodal 50 100 25 50 100 25 50 100 Zn(II) (M) 50 0.02 100 0.02 25 0.02 50 0.02 100 0.02 25 0.02 50 0.02 100 0.02 10 25 25 0.02 11 50 50 0.02 12 100 100 0.02 1 Particle Size Distribution.PDF Image | Spinning Disk Reactor Nano Production Intensification
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