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Nanomaterials 2020, 10, 1321 5 of 15 Nanomaterials 2020, 10, x FOR PEER REVIEW 5 of 15 Figure 2. 3D graph of average nZnO diameter (d [nm]) in function of varied reagent solution flowrate Figure 2. 3D graph of average nZnO diameter (d [nm]) in function of varied reagent solution flowrate and r . and ri.i 3.2. Influence of Disk Rotational Velocity and Reagent’s Concentration 3 0.02 0.02 0.08 0.08 1400 1400 1.5 1.5 67.1 74.3 0.949 0.445 Unimodal Table 2 reports the detail of the results obtained in the first 12 runs. Figure 3 reports the average diameter of nZnO measured at different ω (a) and Zn(II)/KOH molar concentrations at 0.05 L/min (bT)abanled2.0R.5esLu/mltsinob(tca)i.ned in the first 12 runs. ID 1 2 Table 3 reports the detail of the results obtained in the remaining 13 runs. P (kg/d) 0.113 0.224 PSD Unimodal Unimodal QZn (L/min) QKOH (L/min) Zn(II) (M) KOH (M) w (rpm) ri (cm) d (nm) Yield 1 25 25 50 50 100 100 0.02 0.08 1400 1.5 84.2 Table 3. Results obtained in the remaining 13 runs. 0.961 0.956 ID QZn (L/min) QKOH (L/min) 25 25 Zn(II) (M) KOH (M) w (rpm) ri (cm) d (nm) 81.3 Yield P (kg/d) 0.115 PSD 1 4 0.02 0.08 1400 2 0.980 Unimodal 13 50 50 0.02 0.08 200 2.5 68.4 0.979 0.23 Bimodal 5 50 50 0.02 0.08 1400 2 64.1 0.972 0.228 Unimodal 14 50 50 0.02 0.08 400 2.5 62.4 0.979 0.23 Bimodal 6 100 100 0.02 0.08 1400 2 69.5 0.966 0.453 Unimodal 15 50 50 0.02 0.08 800 2.5 58.5 0.985 0.23 Bimodal 16 50 50 0.02 0.08 1200 2.5 54.1 0.992 0.23 Unimodal 7 25 25 0.02 0.08 1400 2.5 69.1 0.982 0.116 Unimodal 17 50 50 0.2 0.8 1400 2.5 54.2 0.992 2.32 Unimodal 8 50 50 0.02 0.08 1400 2.5 50.3 0.979 0.229 Unimodal 18 50 50 0.1 0.4 1400 2.5 53.1 0.991 1.16 Unimodal 9 100 100 0.02 0.08 1400 2.5 55.7 0.968 0.454 Unimodal 19 120 50 50 0.05 0.0.25 0.2 0.028 1400 11400 2.5 50.9 0.993 0.58 Unimodal UnUimnimododaall 21 50 50 1 4 1400 2.5 60.4 0.991 11.60 Bimodal 11 50 50 0.02 0.08 0.08 1400 3 59.4 0.956 0.230 Unimodal 22 500 500 0.5 2 1400 2.5 56.1 0.983 57.60 Unimodal 12 100 100 0.02 1400 3 63.7 0.952 0.456 Unimodal 23 24 25 500 500 500 500 500 500 0.75 1 1 Particle4Size Dis1t4ri0b0ution.2.5 2 8 1400 2.5 64.7 1 Particle Size Distribution. 2550 250 23.5 7565..46 0.09.69911 0.151.681 3 1400 2.5 59.4 62.3 0.981 0.982 0.983 86.22 115.08 230.39 Unimodal Bimodal Bimodal 3.2. Influence of Disk Rotational Velocity and Reagent’s Concentration Figure 3 reports the average diameter of nZnO measured at different ω (a) and Zn(II)/KOH molar concentrations at 0.05 L/min (b) and 0.5 L/min (c).PDF Image | Spinning Disk Reactor Nano Production Intensification
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