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Optimisation of the parameters is trivial with a SDR; the hold-up is small so that, depending on the property of the product being analysed and the analytical technique, individual experimental settings can be examined at the rate of several per experimental hour. Thus, a comparison of the GPC for the products from the two processes (Figure 7) was taken as an indication of the similarity of the products. It should be noted that this comparison involves a well established technical batch process which has been optimised. Figure 7. A Comparison of the GPC for the Products from the Batch STR and the SDR whose Properties are given in Table 1 For the preparation of SPU we attached a static mixer to the outlet of the SDR into which the amino silane and stabiliser was dosed according to the flow in the SDR. A typical GPC of the products obtained compared with that from an optimised commercial product (produced in a batch STR) is shown in Figure 8. Time (minutes) Figure 8. A Comparison of the GPC for the SPU Products from the Batch STR and the SDR 7 IntensityPDF Image | Spinning Disk Reactor for Polymers and Nanoparticles
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