Spinning Disk Reactor for Polymers and Nanoparticles

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Spinning Disk Reactor for Polymers and Nanoparticles ( spinning-disk-reactor-polymers-and-nanoparticles )

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Preparation of Silver Nano-Particles An aqueous AgNO3-solution was mixed with the polyol and fed to the centre of the disc at the desired rate. The disc was preheated to temperatures between 120 and 200 oC and the disc speed varied between 200 and 2500 rpm. The silver particle dispersions were collected continuously. Acknowledgements: The authors would like to thank BASF and Degussa for their support of this work and their agreement, especially with respect to Fig. 6-10, that it can be published. Keywords: nanoparticles; photopolymerization; polyurethanes; spinning disk reactor; step-growth-polymerization _________________________________ [1] A. Stankiewicz, UEF conference “Refocusing Chemical Engineering”, Barga/Italy, (May 27- June 1, 2001) [2] A. Stankiewicz, J .A. Moulijn, Re-Engineering The Chemical Processing Plant, Marcel Dekker New York, 2004, 3 (Fig. reproduced with permission of TAYLOR & FRANCIS GROUP LLC – BOOKS.) [3] J. Elkington, Cannibals with Forks. The triple bottom Line of 21st Century Business, Capstone Publ. Ltd., Oxford, UK, 1997 [4] DSM Magazine 1999, 148, 4 (Fig. Reproduced with permission from SABIC.) [5] A. Aoune, C. Ramshaw, Int. J. Heat & Mass Transfer, 1999, 42, 2543 [6] K. P. Jäckel in W. Ehrfeld(Ed.), Microsystem Technology for Chemical and Biological Reactors, Dechema Monograph 1995, 132, 29 [7] W. Siemes, Grundbegriffe der Verfahrenstechnik, Hüthig, Heidelberg, 1966,133 [8] N. C. Jacobsen, PhD thesis TU München, 2011, 76 [9] M. Dehkordi, Chem. Eng. Process.2002, 41, 251 [10] G. S. Laddha, T. E. Degalessan, Transport Phenomena in Liquid Extraction, McGraw- Hill, New Delhi, India, 1976 [11] R. E. Treybal, Liquid Extraction, McGraw-Hill Book Co., New York, 1951 [12] C. Ramshaw, R. J. J. Jachuck, (Protensive Ltd, Cambridge, UK), US 6972113, 2005 [13] Z. Cai, PhD thesis, Technische Universität, München, 2008 [14] C.M. Ong, S. Pask, S. Guo, F. Mersmann , (Lanxess Deutschland GmbH), US 7666950, 2010 [15] R. Lemmerz, 2nd European Congress on Adhesives and Sealants Raw Materials 2001, Silan-terminierte Polyurethane als Bindemittel für Klebstoffe imBaubereich; [16] H. Mack, 2nd European Congress on Adhesives and Sealants Raw Materials 2001, Silanvernetzende Polyurethane: Technologietrends; [17] A. Ram, Fundamentals of Polymer Engineering, Plenum Press, New York 1997, 1-30 [18] S. F. Sun, Physical Chemistry of Macromolecules, 2ndEd. Wiley, Hoboken, NJ, 2004, 19-24 15

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