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Nanomaterials 2020, 10, 638 7 of 17 3.2.3. X-ray Diffraction (XRD) Crystalline properties of biosynthesized nanoparticles were evaluated using XRD (Figure 2B). Main diffraction peaks identified in the diffractogram were at 2θ values of 27.9◦, 32.4◦, 46.2◦, 54.8◦, 57.6◦, 67.5◦, 74.3◦, and 76.9o. They corresponded to (111), (200), (220), (311), (222), (400), (331), and (420) planes, part extracts of the P. vulgaris plant. 3.2.4. Transmission Electron Microscopy (TEM) 3.2.4. Transmission Electron Microscopy (TEM) (B) respectively, and confirmed the face-centered cubic (FCC) structure of AgCl according to the database of Joint Committee on Powder Diffraction Standards (JCPDS), file number 31-1238. XRD analysis confirmed that biogenic AgCl-NPs were synthesized [11]. According to the Debye–Sherrer equation, Figure 2. (A) The FTIR spectrum and (B) the XRD pattern of biosynthesized AgCl-NPs using aerial the average crystalline size of biosynthesized AgCl-NPs was 28.6 nm. TEM analysis (Figure 3A,B) clearly confirmed that the shape of biosynthesized AgCl-NPs was TEM analysis (Figure 3A and B) clearly confirmed that the shape of biosynthesized AgCl-NPs spherical, while their size was ranged from 14.3 to 50.7 nm with the average of 28.6 ± 9.0 nm—that was spherical, while their size was ranged from 14.3 to 50.7 nm with the average of 28.6 ± 9.0 nm— being the same as the particle size measured based on the XRD pattern. that being the same as the particle size measured based on the XRD pattern. (A) Figure 3. Cont.PDF Image | Synthesis of Biogenic Silver Nanoparticles Aerial Part Extract
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