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20 Results and discussion Figure 3.1: SEM images of the NaX films grown in the gel (a, c, e) and in the clear synthesis solution (b, d, f). Arrows indicate aggregates of crystals deposited from the bulk of the synthesis solution by sedimentation. synthesis mixture. The data show that the samples are comprised of randomly oriented NaX and cordierite crystals, and the intensity of the NaX zeolite peaks is highest for the film grown in the gel, in accordance with the weight gain. Figure 3.3 (a) shows a top-view SEM image of a ZSM-5 film grown in a template-free synthesis gel on a 400 cpsi cordierite monolith. The film consists of well intergrown crys- tals and has an average thickness of 1.9 μm, see Figure 3.3 (c) and Table 3.1. AlthoughPDF Image | Structured Zeolite Adsorbents for PSA Applications
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