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The catalyst coating was chosen to be Rh/TiO2, specifically a 5.5 wt% washcoat loading of 2.5 wt% Rh on TiO2. Rhodium was chosen for the active phase due to its reported performance in other experimental systems studying CO2 dissociation. For example, a study performed by [8] compared the effects of different rare metal catalysts on CO2 dissociation when coated inside an AC glow discharge reactor at atmospheric pressure. A mixture of 2.5% CO2 in He was passed through the plasma creating CO and O2 with 80% selectivity. Of the different metal catalyst coatings used, rhodium had the highest reactivity, followed by platinum, copper, paladium, and silver. The CO2 conversion efficiency as a function of mass flow rate is shown in Figure 5.9, while the energy efficiency is given in Figure 5.10. It is evident that Rh consistantly achieved the highest conversion degree over the other metals, and had the highest energy efficiency for the highest CO2 flow rate tested. Figure 5.9: CO2 conversion efficiency for 2.5% CO2 in He mixture. [8] The catalyst support, TiO2, was chosen for its reported ability to increase CO2 activation. Specifically an experimental investigation was done by [76] comparing CO2 dissociation on different nickel supported catalysts Ni/Al2O3, Ni/SiO2, and Ni/TiO2. The rate constant of dissociation was experimentally determined for the reaction over 91PDF Image | CO2 Conversion in a Microwave Plasma Catalyst System
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