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Analysis of the C2 spectra indicates that the microwave plasma does not produce a complete non-thermal plasma when operating with CO2 as a major gas species. The vibrational and rotational gas temperatures are in thermal equilibrium, leading to low values of energy efficiency. 7.1.3 Plasma/Catalyst System Characterization The plasma/catalyst system was characterized to determine the influence of the monolith structure and the Rh/TiO2 catalyst material on CO2 dissociation. Both the monolith and the catalyst resulted in changes to efficiencies and plasma temperatures. The monolith structure causes a slight efficiency loss for CO2 dissociation The plasma temperatures at the discharge center move closer towards thermal equilibrium with the presence of the monolith downstream The monolith structure impedes exiting gas flow due to a 43% reduction in tube cross-sectional area, most likely resulting in higher pressure upstream of the monolith and leading to lower efficiencies. The monolith structure is not an appropriate design for this experimental system with high gas flow rates at atmospheric pressure. The Rh/TiO2 catalyst coating causes a large drop in dissociation efficiency for this experimental configuration. The catalyst can be plausibly said to enhance the reverse reaction CO + O2 → CO2 + O, resulting in an increased flow of CO2 exiting the discharge tube. The Rh/TiO2 coating is not an appropriate catalyst to facilitate CO2 dissociation under high gas temperature conditions at atmospheric pressure 155PDF Image | CO2 Conversion in a Microwave Plasma Catalyst System
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