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When the feed was saturated with air, the decomposition rate increased dramatically, as seen in Figure 12. Residues found in the reactor after the decomposition experiments (Figure 13) were examined by a number of different techniques. The mass of the residues increased with experimental temperature, but was lower at the same temperature when the feed was saturated with air. Analysis of the residues suggested that the residues were primarily heavy saturated hydrocarbons. Open valve to BPR TC Furnace Reactor SV Sample Collection PT ToVent or Overflow RV Flow Meter PT Pressure Transducer RV Relief Valve SV Switching Valve Check Valve Recirculation Pump ToVent or Overflow RV He He Pressure Regulator 22 ToVentor 1 1 3 Overflow 3 4 4 HP Syringe Pump Cyclo- pentane SV2 SV1 Figure 8. Schematic of the organic fluid decomposition test system. 80 70 60 50 40 30 20 10 - Figure 9. Total decomposition products as a function of time on stream (240°C, 43 bars). Compound Propylene Butanes Pentene Cyclopentene Hexanes/Hexenes Heptane/Heptene Octane/Octene Concentration (ppm) 2 14 16 20 9 4 5 0 50 100 150 200 250 300 Elapsed Time (Hours) 11 Table 3. End of run compounds and concentrations (240°C, 43 bars). Total Decomposition Products (ppm)PDF Image | Final Report Modifications and Optimization of the Organic Rankine Cycle to Improve the Recovery of Waste Heat
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