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3.3.2. Recycling of Polyetheretherketone Composite Materials.....................................88 3.3.3. Decomposition and Recycling of Polyepoxide Thermoset Resin...........................95 3.3.4. Processing and Characterisation of Carbon Fibre ...............................................103 3.3.5. Recycling of Carbon Fibre Reinforced Polyepoxide Composite Materials ..........108 3.4. Analytical Techniques .................................................................................................109 3.4.1. Confirmation of PEEK Amorphicity ......................................................................109 3.4.2. Analysis of Supercritical Carbon Dioxide Processed PEEK...................................114 3.4.3. Analysis of Polymer Decomposition Products .....................................................121 3.4.4. Analysis of Carbon Fibre ......................................................................................131 3.4.5. Analysis of Carbon Fibre Reinforced Polymeric Materials ..................................150 Chapter 4. Results Part A: Processing and Recycling of Polyetheretherketone....................152 4.1. Supercritical Carbon Dioxide Processing of Polyetheretherketone ...........................152 4.1.1. Confirmation of Amorphicity ...............................................................................152 4.1.2. Effects of scCO2 Processing on the Polymer Transitions .....................................161 4.1.3. High-Pressure Differential Scanning Calorimetry ................................................168 4.1.4. Carbon Dioxide Containment with PEEK .............................................................172 4.2. Decomposition and Recycling of Polyetheretherketone Composite Materials .........179 4.2.1. Ethanol and Water Co-solvent System ................................................................179 4.2.2. Propanol and Water Co-solvent System..............................................................199 4.2.3. Acetone and Water Co-solvent System ...............................................................207 10PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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