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LIST OF FIGURES Figure 1: Phase diagram for water, showing the triple and critical points, equilibrium data obtained from National Institute of Standards and Technology (NIST) and [1]. Solid lines represent phase transitions.....................................................................................................36 Figure 2: Structure of poly(oxy-1,4-phenyleneoxy-1,4-phenylelecarbonyl-1,4-phenylene) PEEK .........................................................................................................................................75 Figure 3: Left; 2,2-Bis[4-(glycidyloxy)phenyl]propane (DER 332, BADGE), Right; 4,4’- diaminodiphenyl sulfone (DDS) ...............................................................................................76 Figure 4: Low-Temperature Reactor (LTR) system showing a; complete setup, b; sapphire viewing windows......................................................................................................................79 Figure 5: High-Temperature Reactor (HTR), 100 ml nominal volume, a; Side profile showing identification markings (Hastelloy), b; top-view showing internal volume (Hastelloy), c; complete setup (stainless-steel)..............................................................................................81 Figure 6: High-Temperature Reactors showing the discolouration at the end-of-life of the reactor, Hastelloy (left), stainless-steel (right) ........................................................................82 Figure 7: D.E.R. 332 DDS Polyepoxide curing cycle, all dynamic segment rates = 1 K min-1 ...98 Figure 8: Bespoke carbon fibre alignment tool, stainless steel, approximately 120 mm in length .....................................................................................................................................107 Figure 9: DSC method 1; Determination of percentage crystallinity (%XC)...........................112 Figure 10: HPDSC Method 1, analysis of PEEK melting process under CO2 pressure environment ..........................................................................................................................115 Figure 11: HPDSC Method 2, single dynamic segment with a slow heating rate to investigate the impact of CO2 on Tg, TC and Tm ........................................................................................116 Figure 12: HPDSC Method 3, minimal heating rate for maximum thermal equilibrium.......117 13PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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