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Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials

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Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials ( supercritical-fluids-and-their-application-recycling-high-pe )

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Table 13: Reaction schedule for the investigation of carbon chain-length on the decompositon of thermoset epoxy resin...............................................................................103 Table 14: Carbon fibre processing control sample generation .............................................105 Table 15: Reaction schedule for the investigation of the effect of co-solvent [Co-solvent] concentration on the tensile strength of carbon fibres. [Cs2CO3] = 0 mg ml-1......................106 Table 16: Specific investigation of effects of [Cs2CO3] in conjunction with co-solvents on the physical properties of carbon fibres ......................................................................................107 Table 17: Reaction schedule for initial investigation into the decomposition of commercially available carbon fibre reinforced polymers...........................................................................109 Table 18: HPLC mobile phase compositions for the quantitative analysis of polymer decomposition products........................................................................................................128 Table 19: HPLC Standard concentrations used to prepare the required calibration curve ..130 Table 20: Impedance as a function of frequency for a single carbon fibre 85 mm in length138 Table 21: Comparison between carbon fibre diameter as calculated by EIM and measured by SEM for multiple carbon fibres..............................................................................................140 Table 22: Limit of Detection (LOD) for determination of number of fibres in a bundle by EIM ................................................................................................................................................ 148 Table 23: EDX Analysis of solid deposits after 0 and 60 minute reactions (conditions as in figure 57)................................................................................................................................192 Table 24: Phenol concentration [PhOH] in organic and aqueous fractions, produced by the decomposition of epoxy resin. T = 573 K, tr = 30 min, [Cs2CO3] = 10 mg ml-1 .......................237 Table 25: XPS binding energy of specific functional groups ..................................................265 Table 26: Initial findings for the recycling of commercially available CFRP's........................271 26

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