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700 650 600 550 500 450 400 350 0 50 100 150 200 250 300 Time (min) Figure 12: HPDSC Method 3, minimal heating rate for maximum thermal equilibrium HPDSC Method 3 was designed to provide low-noise data across all polymeric transitions. Although it initially appears similar to HPDSC Method 2 (Figure 11) the starting temperature is 400 K, followed by a 5 min isothermal segment. The sample is then heated to 673 K at 1 K min-1 in an attempt to maximise the thermal equilibrium between the CO2 and the thermocouple. 117 Temperature (K)PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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