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700 600 500 400 300 200 0 5 10 15 20 Time (min) Figure 14: HPDSC Method 5, rapid heating through all polymeric transitions Tg, TC and Tm HPDSC Method 5 (Figure 14) consists of a single dynamic segment heating from 298 K to 673 K at 20 K min-1. Contrary to HPDSC Methods 1 – 4, it is designed to minimise the thermal equilibrium between the thermocouple and the CO2. In doing so, it is likely that only the CO2 adjacent to the sample and reference pans is close to the temperature of the sample. Having a relatively high heating rate it may be possible to alleviate, to some extent, the effects of CO2 turbulence. Fourier Transform Infra-Red Spectrometry FT-IR Method 2 FT-IR spectrometry was used identify the functional groups associated with PEEK as well as to investigate the presence of CO2 trapped within the polymer matrix. Each spectrum 119 Temperature (K)PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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