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coated with gold using an Emscope SC 500 Sputter Coater (Quorum Technologies, UK) prior to being loaded into the SEM. When required Energy Dispersive X-Ray Spectrometry EDX analysis was carried out using an Inca X-Sight (Oxford Instruments, UK). Although the method of analysis is non-destructive with respect to the sample it was not possible to recover the samples analysed by SEM and SEM-EDX for further analysis due to the sample preparation process. Gas Chromatography – Mass Spectrometry Gas Chromatography – Mass Spectrometry (GC-MS) was used to perform separation and identification of decomposition products. A Waters Corporation GCT Premier GC-MS system (Waters Corporation, USA) was used in conjunction with necessary column to perform the required separation. The method is specific to the column type and therefore methods are presented according to the column used. In preparation for GC-MS, approximately 1.5 ml of reactor extract was filtered, to remove any suspended fines, and collected into standard GC vials. The initial method utilised a ZB5-MS column (Phenomenex, USA) and is shown in Figure 18. 125PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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