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100 90 80 70 60 50 40 30 20 14 16 18 20 22 24 26 28 30 32 34 36 2(O) Figure 36: WAXS Spectrum for PEEK150PF post quenching from melt phase Inspection of Figure 36 shows that the well-defined peaks, derived from the scattering by polymer crystallites, are not observed for quenched samples. Small deviations from the generally broad peak generated by the amorphous PEEK are identified. From these data it may be inferred that the sample is largely amorphous, and when combined with the information obtained by DSC and FT-IR, the samples are considered to not contain sufficient crystallinity to impede the investigation into the effects of scCO2 processing carried out in this research. Having determined the amorphicity of the PEEK samples produced by quenching from the melt phase, attention is now directed towards investigating the effects of scCO2 on the bulk polymer. 4.1.2. Effects of scCO2 Processing on the Polymer Transitions 161 Intensity (cps)PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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