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12 10 8 6 4 2 0 -2 -4 -6 -8 300 400 500 600 Temperature (K) Figure 41: HPDSC thermogram for amorphous PEEK in-situ measurement, PiCO2 = 3.0 MPa, HPDSC method 5 Figure 41 shows that the in-situ measurement of the effects of CO2 on the polymer transitions is possible, with limited success, by means of HPDSC. The crystallisation and melting temperatures are prominent and easily identified. The glass transition temperature however is obscured by noise introduced by the use of CO2, as discussed in Chapter 3.4.2. The crystallisation temperature during the in-situ measurement was reduced from 449 K to 443 K, in accordance with the post processing analysis discussed previously. The melt temperature increased by 3 K, further indicating that the potential for high-pressure CO2 to force the molecular chains together. Increasing the CO2 pressure further significantly increases the noise as shown in Figure 42. 170 Heat Flow (mW)PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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