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loading by BuOH. Consequently the reaction pressure increased, enabling BuOH to attain the critical point and the subsequent increase in diffusivity. This can be observed in Figure 92. 12 10 8 6 4 2 0 H2O [BuOH] = 10 %v [BuOH] = 20 %v [BuOH] = 50 %v [BuOH] = 80 %v BuOH + = [BuOH] Tc, Pc 300 350 400 450 500 550 600 Temperature (K) Figure 92: Reactor internal pressure as a function of temperature for [BuOH] = 0 - 100 %v, tr = 30 min, [Cs2CO3] = 10 mg ml-1, + = critical point Examination of Figure 92 shows that only in the case of 100 % BuOH is the supercritical fluid phase transition observed. It should be noted that the pressure recorded is that of the reactor and is the sum of the partial pressures of the individual components. When miscible fluids are used, such as ethanol and water, there is a single transition to the supercritical phase. However, in the case of immiscible fluids it is possible for one fluid to attain the supercritical state whilst the second fluid remains subcritical. In such instances, deviation from the pressure / temperature correlation observed prior to the critical point is less pronounced and more difficult to identify. This is the case presented in Figure 92 where 235 Pressure (MPa)PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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