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in Figure 102. The detection of gold is a result of the sputter coating of the sample, necessary due to epoxy resin being an electrical insulator. C O Au Au Cs Cs Cs 0123456 keV Figure 102: EDX Analysis of solid deposits on the surface of epoxy resin post-processing Having a lower solubility, and subsequent reduction in Cs2CO3 concentration compared to the ethanol system, the catalyst concentration within the bulk polymer will be lower. This in turn leads to a reduction in the percentage decomposition for a given reaction time. Figure 101 ‘c’ shows that after a reaction time of 10 minutes some fragmentation is visible; Figure 101 ‘d’ shows an area of surface removal exposing a secondary layer. The surface layer is highly porous with the exposed area showing a macro-porous cell structure. The progression of the reaction on polymer degradation is shown in Figure 103. 250PDF Image | Supercritical Fluids and Their Application to the Recycling of High-Performance Carbon Fibre Reinforced Composite Materials
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