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concentratiOn of hydrazme sulfate has been determmed, no further adjustment should be necessary 74 Place appropnate mtrate standards m the sampler m order of decreasmg concentratiOn ofmtrogen CompleteloadmgtraywIthunknownsamples 7 5 For both the AAI and theAAII use a 2 mmute samphng rate 8 CalculatiOn 8 1 Prepare a standard curve by plottmg peak heIghts ofprocessed standards agamst known concentratiOns Compute concentratiOns of samples by companng sample peak heIghts wIth the standard curve 9 PreclSlon and Accuracy 9 1 In a smgle laboratory usmg dnnkmg water, surface water and mdustnal waste at concentratiOns of 039, 1 15, 176 and 475 ug NOr N/l, the standard devIations were ±O 02, ±O 01, ±O 02 and ±O 03, respectIvely In a smgle laboratory usmg dnnkmg water at concentratiOns of0 75 and 297 the recovenes were 99% and 101% BIblIography 1 Kamphake, L , Hannah, S , and Cohen, J , "Automated AnalysIs For NItrate by Hydrazme ReductiOn", W ater Research 1,205 (1967) 353 1-3PDF Image | Methods for Chemical Analysis of Water and Wastes
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