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These films were used as received. Waterborne PU dispersion (BondthaneTM UD-615) was obtained by the courtesy of Bond Polymers International. PU film (50 μm) was made by spin-coating the dispersion onto the substrate. Ag NWs dispersion (Agnw-L70) was purchased from ACS Material. Isopropyl alcohol (IPA) 99% was purchased from VWR. 2.4.5.2 Fabrication of PPHA films PPHA films were formulated in a clean scintillation vial by dissolving all solid contents (i.e., PPHA, PAG, anthracene) and liquid contents (BMP TFSI) in THF. Weight ratio of 12:1 for THF and PPHA were used for all formulations in order to obtain the viscosity to spread and cover the PTFE petri dishes for drying. All polymer formulation was prepared containing 10 part per hundred resin (pphr) PAG, 2.1 pphr anthracene, and 100 pphr BMP TFSI, with all weight fraction referenced to the weight of PPHA added into the formulation. The sample was dried in a nitrogen-rich, pressurized chamber at 15 psig for 18 hours, followed by slow bleeding of THF out of chamber to relieve head pressure for 3 hrs. Samples were then taken out of the pressurized chamber and peeled off the substrate. All samples were then flattened and allowed further drying for 3 days before taken to test. All dried samples have an average thickness of 100 μm. 2.4.5.3 In-Situ ATR-IR Characterization of PPHA Films The degradation of 100 μm thick PPHA films was characterized by a Nicolet iS50 FT-IR instrument. Attenuated total reflectance (ATR) mode was used and total scans of 32 were performed for each sample. Samples were exposed using a portable B-100 series UV lamp with an intensity of 4 mW/cm2 at 365 nm. Data were collected after samples were 71PDF Image | HIGH PERFORMANCE TRIBOELECTRIC NANOGENERATOR AND ITS APPLICATIONS
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