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Figure 8. a) Schematic of the phase transformation process of MoS2 nanosheets using SC CO2. b) HRTEM image of the lateral heterostructures of MoS2. c,d) Two filtered images of 2H-MoS2 and 1T-MoS2, respectively. Reprinted from reference [51]. Copyright 2016, American Chemical Society. Figure 9. Schematic diagram of the phase transformation mechanism of few-layered MoS2 in CO2/PVP/H2O system. Reprinted from reference [52]. Copyright 2017, Wiley-VCH. van der Waals forces) and lateral (grown together seamlessly in plane by covalent bonds) heterojunctions.[55–58] Recently, van der Waals heterostructures have been fabricated via either top-down approaches associated with exfoliation of bulk materials or bottom-up approaches such as solution-based synthesis and CVD-based growth. Jeffery et al.[59] prepared the layered MoS2-WS2 hybrids by flocculating a mix- ture of the colloidal dispersions of ammoniated MoS2 and WS2, but the colloidal dispersions would be contaminated easily and the layers could be restacked randomly. Azizi et al. created two atomically thin free- standing van der Waals heterostructures systems by CVD methods: epi- taxial growth of monolayer WSe2/graphene and nonepitaxial growth of MoS2/grapheme heterostructures. This study revealed the significant role of defects on the heterostructure growth, and photoluminescence (PL) measurements showed a significant PL quenching of TMDs on suspended graphene.[60] For lateral heterostructures, Ci et al.[61] syn- thesized uniform and continuous h-BNC films consisting of hybridized Energy Environ. Mater. 2018, 1, 46–60 52 © 2018 Zhengzhou UniversityPDF Image | CO2 and 2-Dimensional Nanomaterials with Green Chemistry
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