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GREEN CHEMISTRY CO2 extraction Limonene Orange Rind

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GREEN CHEMISTRY CO2 extraction Limonene Orange Rind ( green-chemistry-co2-extraction-limonene-orange-rind )

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3. Extraction. Fill a PLASTIC graduated cylinder two-thirds full with hot tap water (40-45° C) and place it under the hood. Fill the centrifuge tube with finely crushed dry ice, tapping the bottom of the tube on the counter and adding more ice until the tube is full, then cap the centrifuge tube quickly and tighten it until the cap stops twisting. Be careful not to close it too tightly or the tube may explode. Lower the full centrifuge tube tapered end first into the graduated cylinder water bath waiting in the hood. Pull the hood safety glass down as soon as you place the centrifuge tube into the warm water bath. The dry ice should become liquid CO2 after a minute and remain in the liquid phase for about 3 minutes until all the gas has seeped out the top. If the CO2 has not entered the liquid phase after 2 minutes, the centrifuge tube did not have a tight enough seal, and either the cap and tube should be replaced, or the dry ice was left in the tube too long without sealing the cap on. After all the liquid CO2 is gone, uncap the tube. If necessary, rearrange the solid orange peel before the second extraction. A piece of wire can be used to break up the solid mass and create a channel to the bottom for liquid CO2. . Repeat the extraction by refilling the tube with dry ice, resealing the cap and putting the tube back in the water. Carefully remove the solid and the trap by pulling the wire handle with tweezers. Pre-weigh a small sample vial before collecting the extracted oil in it, and reweigh the vial after the oil has been collected. Lab #7 Report Sheet Name___________________________ 1. Calculate the mass percentage recovery of the oil from the original amount of orange rind used. 2. Write a half page discussion regarding your thoughts about supercritical CO2 extraction as an example of green chemistry. Find the part of this topic that interests you the most and write about it!

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