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Extraction of Bio-Butanol using Supercritical Carbon Dioxide

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Extraction of Bio-Butanol using Supercritical Carbon Dioxide ( extraction-bio-butanol-using-supercritical-carbon-dioxide )

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solvent residues and limiting thermal degradation (Vázquez da Silva, Barbosa, & Ferreira, 2002). Figure 2.5: CO2 phase diagram (Modified from The Freezing Point And The Dew Point – Part 2. (2010)) 2.4 Supercritical Fluid Extraction Equipment The basis of supercritical fluid extraction equipment starts with the reaction and separation operations. Typically a system that will create and extract butanol, or other products in a similar situation, would have two different functions consisting of reaction vessels and separation vessels. This can be carried out using a variety of different equipment including packed bed reactors, distillation columns, membrane separators, etc. One of the main reasons the processes are separated is due to the different conditions that are needed for the different unit operations. For example, an endothermic reaction might require vessels specified for high temperatures, but then to use distillation to separate the multiple products it could require a lower temperature. These separate parameters force the reaction and separation processes to be distinctly different. However, there are certain situations where reaction and separation can occur within the same range of parameters and these processes can be capitalized upon to create a more efficient system. 24

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