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LIMITS OF SMALL SCALE PRESSURE SWING ADSORPTION

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LIMITS OF SMALL SCALE PRESSURE SWING ADSORPTION ( limits-small-scale-pressure-swing-adsorption )

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controllers (BPC) placed at various points in the process. BPC1 was used to control the adsorption pressure and BPC4 was used to control the desorption pressure. Flow rate in the system was measured by three MKS flow meters located at three separate points in the process. One is on the feed line (FC1 on Figure 5.6), another on the purge line (FC2 on Figure 5.7), and a third on the exit manifold (FC4 on Figure 5.5). There is an additional Omega FDMA-1600A Gas Flow Meter (FLOWTRNS on Figure 5.7) used to measure mass flow rate, pressure, and temperature for the equalization flow exclusively. Due to slow response time, all flow controllers were left open and used only as flow meters. Inlet flow was controlled through a needle valve after FC1. A needle valve (NEEDLVAL on Figure 5.7) was placed before FC2 to control purge flow into the columns. Exit flow composition is measured by an AMI (Advanced Micro Instruments) Oxygen Analyzer (O2ANALYZ on Figure 5.5) located on the product end of the process within the exit manifold. There are also ports (MS1, MS2, MS3, MS6) at both ends of each column for capturing a small amount of gas to analyze in a mass spectrometer. These ports were only used if the mass spectrometer was required for fine tuning of a process. Data collection from pressure transducers, flow controllers, and the oxygen analyzer was done with a National Instruments 7025E data acquisition system. The data was then displayed on a computer using Lab Windows software. The software was also used to record the data into a comma-separated-value file for further analysis. 84

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