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Figure 5.11: RGA calibration curve for capillary configuration. 5.4.2 Optical Emission Spectroscopy The Ocean Optics HR4000 spectrometer is used to take optical emission spec- troscopy (OES) data, capable of measuring emission in the range of 200-1100 nm. With the insertion of a 5 micron slit, data is taken in the visible region from 400 nm - 800 nm with an optical resolution of 0.22 nm at full width at half maximum (FWHM). An Ocean Optics 74-UV fused silica collimating lens with a range of 200-2000 nm is attached to an optical fiber cable 400 microns in diameter which transmits light to the spectrometer. When focused for collimation, beam divergence is 2°or less, depending on fiber diameter, and the lens can be adjusted for UV-VIS or VIS-NIR setups. The collimating lens is mounted on the cylindrical waveguide hole in the position closest to the center of the plasma, where emitted visible light is at its brightest. An illustration of the OES setup is shown in Figure 5.12. Due to the wavelength restrictions of the spectrometer, the C2 Swan Band system is the only molecular spectra observed during experiments. Thus all OES analysis is completed using the C2 system. The spectrometer was calibrated for wavelength using an Ocean Optics HG-1 94PDF Image | CO2 Conversion in a Microwave Plasma Catalyst System
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