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Figure 5.12: Optical emission spectroscopy setup. mercury-argon lamp as instructed by the spectrometer manual. An intensity calibration was performed using a tungsten filament as a blackbody source. Approximately 3.6-3.8 A of current flowed through the filament, resulting in an operating temperature of around 3000 K for the filament. The relative intensity spectrum of the filament was captured by the spectrometer and used to calculate an intensity calibration factor, Q. Since the tungsten filament can be treated as a blackbody source, Planck’s blackbody radiation equation (5.5) can be used to plot the actual blackbody curve for tungsten. (5.5) Here I is intensity, h is Planck’s constant, λ is wavelength, and T is the temperature of the tungsten filament. The calibration factor, Q, can be found by taking the intensity ratio of the true (calculated) tungsten blackbody curve to the measured relative tungsten spectrum recorded by the spectrometer. Thus to find the true intensity of any recorded spectrum, the recorded relative emission intensity must be multiplied by Q. Figure 5.13 demonstrates the difference between a relative spectrum and the 2hc2 1 I= 5 · hc λ eλkT −1 95PDF Image | CO2 Conversion in a Microwave Plasma Catalyst System
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